Process for the preparation of 1,3,5-trifluoro-2,4,6-trinitroben

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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C07C 7912

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041735919

ABSTRACT:
A process for producing 1,3,5-trifluoro-2,4,6-trinitrobenzene by:

REFERENCES:
patent: 4032377 (1977-06-01), Benziger
Siele, Victor I. and Matsuguma, Harold J.; "Investigation of Synthetic Meds for Preparing the Fluoro Derivatives of Symmetrical Trinitrobenzene," Technical Report 2682, (Picatinny Arsenal, Dover, N.J., 1960).
Shaw, G. C., III, and Seaton, D. C.; "The Synthesis of Some Fluorine-Containing Trinitrobenzenes," J. Org. Chem., 26, 5227 (1961).
"Research on Fluorochemicals," ASD Technical Documentary Report No. ASD-TDR-62-111, Jul. 1962; Project No. 2858, Denver Research Institute.
Kaplan, Lloyd A., and Taylor, Francis, Jr., "Process Development Study of 1,3,5-Triamino-2,4,6-Trinitrobenzene," NAVORD Report 6017, Mar. 10, 1958.
O'Keefe, David M. and Gurule, Frank M.; "The Synthesis of Symmetrical Trichlorotrinitrobenzene Part 2 -- Nitration with Nitric Acid; Synthesis of By-Products," SAND78-1001 Report, p. 30, Sandia Laboratories, Albuquerque, New Mexico 87185 and Livermore, California 94550, Printed Jun., 1978.

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