Processes for preparing pentafluoroethoxy- and pentafluoroethylt

Organic compounds -- part of the class 532-570 series – Organic compounds – Sulfur containing

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20415777, 20415778, 20415779, 2041578, 20415782, 20415788, 20415792, 260544D, 260544S, 260694, 558423, 558425, 560 18, 560 59, 568 44, 568 52, 568 54, 568 56, 568333, 568588, 568633, C07C14800, C07C 4122

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048373648

ABSTRACT:
A process for the preparation of (pentafluoroethoxy)- and (pentafluoroethylthio)benzene derivatives either from phenol, thiophenol or from halobenzene. A halobenzene is reacted with trifluoroethanol or a phenol or a thiophenol is reacted with a compound of the formula CF.sub.3 --CH.sub.2 --O--R'. The product is chlorinated and the chlorinated product is fluorinated in liquid hydrofluoric acid in the presence of a Lewis acid.
The compounds obtained by the process of the present invention are used as synthesis intermediates in the phytosanitary, pharmaceutical and veterinary industries, and are used in lubricants.

REFERENCES:
patent: 2803665 (1957-08-01), Miller et al.
patent: 3207792 (1965-09-01), Buchanan et al.
patent: 3419595 (1968-12-01), Hansen
patent: 4287125 (1981-09-01), Soula
patent: 4643811 (1987-02-01), Langlois
A. Feiring, J. Amer. Chem. Soc., 44, No. 16 (1979), pp. 2907-2910.

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