Removal of niobium second phase particle deposits from...

Cleaning and liquid contact with solids – Processes – For metallic – siliceous – or calcareous basework – including...

Reexamination Certificate

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C134S003000, C134S026000, C134S028000, C134S034000, C134S035000, C134S036000, C134S040000, C134S041000, C134S042000, C075S715000, C148S254000, C510S488000

Reexamination Certificate

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07468106

ABSTRACT:
The present invention provides a method for removing niobium-rich second-phase-particle (SPP) deposits from zirconium-niobium alloy components. The method comprises washing a freshly pickled and rinsed zirconium-niobium alloy component with an acidified oxalic acid or ammonium oxalate washing solution. The method of the present invention results in a rapid, efficient and complete removal of surface SPP deposits from the zirconium-niobium alloy component without pitting, leaving behind a clean, shiny surface without the need to use water blasting or mechanical wiping operations.

REFERENCES:
patent: 2008/0101527 (2008-05-01), McLaughlin
patent: 2008/0230090 (2008-09-01), McLaughlin et al.
Blumenthal, Warren B., “The Chemical Behavior of Zirconium”, 1958, pp. 191-193, D. van Nostrand Company, Inc., Princeton, New Jersey, USA.

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