Method and device for cleaning desorption ion sources

Radiant energy – Ionic separation or analysis – With sample supply means

Reexamination Certificate

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C436S174000

Reexamination Certificate

active

10757686

ABSTRACT:
The invention relates to the cleaning of contaminated accelerating or guiding electrodes of ion sources used for ion generation by desorption. A cleaning plate is used that has an outer contour similar to that of a standard sample support plate, and may be equipped with cleaning scrubbers that can be moved out when necessary to contact the electrodes. The scrubbers may include soft covers, and can carry out the cleaning by dry rubbing or with the help of high-boiling solvents for the matrix substances. The moving out of the cleaning scrubbers can be controlled by external light pulses from a laser or video camera spot light. Alternatively, the cleaning plate may be equipped with spray nozzles connected to a reservoir of cleaning fluid which is sprayed onto the electrodes, and the evacuation of the ventilated ion source chamber may be used to initiate the spraying.

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patent: 2 317 049 (1998-03-01), None
Donegan et al. “Controlling Matrix suppression for matrix-assisted laser desorption/ionization analysis of small molecules”, Rapid Communicaitons in Mass Spectrometry, 2004; 18: 1885-1888.

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