Preparation of high-purity isobutyramide

Details Preparation of high-purity isobutyramide Preparation of high-purity isobutyramide

1994-12-12

1996-06-04

Kumar, Shailendra

Organic compounds -- part of the class 532-570 series

Organic compounds

Amino nitrogen containing

564133, 564134, 564142, 564215, C07C23102

Patent

active

055234852

ABSTRACT:
A process for preparing high-purity isobutyramide which comprises reacting isobutyryl chloride in toluene or xylene at -15.degree. to 30.degree. C. with ammonia is described.

REFERENCES:
patent: 3901908 (1975-08-01), Fitzi et al.
S. P. Perrine, D. V. Faller, Experientia 49 (1993) 133.
N. O. V. Sonntag, Chem. Revs. 52 (1953) 237.
O. Aschan, Chem. Ber. 31 (1898) 2348.
Organic Synthesis, Coll. vol. III, 490-492, 1955.
G. E. Philbrook (J. Org. Chem. 19 (1954) (623).

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