Organic compounds -- part of the class 532-570 series – Organic compounds – Silicon containing
Reexamination Certificate
2007-10-30
2007-10-30
Barts, Samuel (Department: 1621)
Organic compounds -- part of the class 532-570 series
Organic compounds
Silicon containing
Reexamination Certificate
active
11529591
ABSTRACT:
A sulfide chain-bearing organosilicon compound having the average compositional formula:in-line-formulae description="In-line Formulae" end="lead"?(R1O)(3-p)(R2)pSi—R3—S—(R4—Sm)q—R4—S—R3—Si(OR1)(3-p)(R2)pin-line-formulae description="In-line Formulae" end="tail"?is prepared at low costs and in high yields by reacting a halogen-terminated organosilicon compound having the formula: (R1O)(3-p)(R2)pSi—R3—S—R4—X, sulfur, and optionally a halide having the formula: X—R4—X with an aqueous solution or dispersion of a sulfide M2S or hydrate thereof in the presence of a phase transfer catalyst. R1and R2are monovalent C1-4hydrocarbon groups, R3and R4are divalent C1-10hydrocarbon groups, m has an average value of 2-6, p is 0, 1 or 2, q is 1, 2 or 3, X is halogen, and M is ammonium or alkali metal.
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Barts Samuel
Birch & Stewart Kolasch & Birch, LLP
Shin-Etsu Chemical Co. , Ltd.
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