Preparation of N,N'-bis(2-hydroxyethyl)oxamide

Details Preparation of N,N'-bis(2-hydroxyethyl)oxamide Preparation of N,N'-bis(2-hydroxyethyl)oxamide

1984-11-09

1986-11-11

Warren, Charles F.

Organic compounds -- part of the class 532-570 series

Organic compounds

Amino nitrogen containing

564134, 564136, 564160, C07C10206, C07C10338

Patent

active

046224262

ABSTRACT:
N,N'-bis(2-hydroxyethyl)oxamide is facilely prepared, e.g., in finely divided crystalline form, by reacting an alkyl oxalate with ethanolamine in an aqueous reaction medium.

REFERENCES:
patent: 2857390 (1958-10-01), Kirchner
patent: 3543306 (1970-11-01), Biland
Stuart et al., Can J. Res. 26, pp. 402-409, (1948).
Desseigne, Revue des Poudres, 30, p. 101, (1948).
Knorr et al., Chem. Ber., 36, pp. 1278-1279, (1903).
Rauscher et al., J. Am. Chem. Soc., 70, p. 438, (1948).
Phillips, J. Am. Chem. Soc., 73, pp. 5557-5559, (1951).
D'Alelio et al., J. Am. Chem. Soc., 59, pp. 111-112, (1937).
Wagner et al., Synthetic Organic Chemistry, pp. 568-569, (1953).

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