Process for producing a fluorinated alcohol

Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing

Reexamination Certificate

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C568S840000, C568S841000, C568S843000

Reexamination Certificate

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06894196

ABSTRACT:
A process for producing a high-purity fluorinated alcohol in a good purification yield, is provided.In a process for producing a fluorinated alcohol, which comprises reacting methanol with tetrafluoroethylene or hexafluoropropylene in the presence of an alkyl peroxide, the reaction liquid after completion of the reaction is distilled in the presence of water and HF to separate it into a fraction containing an alcohol derived from the alkyl peroxide and a bottom liquid containing the fluorinated alcohol, and then, the bottom liquid is purified to recover the fluorinated alcohol.

REFERENCES:
patent: 4346250 (1982-08-01), Satokawa et al.
patent: 0 811 594 (1997-12-01), None
patent: 0 968 990 (2000-01-01), None
patent: WO 0114298 (2001-03-01), None
U.S. Appl. No. 10/077,794, filed Feb. 20, 2002, Wada et al.
U.S. Appl. No. 10/131,187, filed Apr. 25, 2002, Okamoto.
U.S. Appl. No. 10/298,652, filed Nov. 19, 2002, Okamoto et al.
U.S. Appl. No. 10/028,827, filed Dec. 28, 2001, Wada et al.
U.S. Appl. No. 10/370,507, filed Feb. 24, 2003, Okamoto.

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