Manufacturing method of carbon nanotubes and laser...

Catalyst – solid sorbent – or support therefor: product or process – Catalyst or precursor therefor – Inorganic carbon containing

Reexamination Certificate

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

C502S182000, C252S503000

Reexamination Certificate

active

06855659

ABSTRACT:
In a manufacturing method of carbon nanotubes by means of laser ablation, carbon molecules having 5-memberd carbon ring bonds (bonds of the pentagon of the fullerenes (C60, C70, C76, etc.)) are included at least in part of the laser irradiation target. By use of such laser irradiation targets, single-wall carbon nanotubes can be formed efficiently in a low temperature process of 500° C. or lower (at 400° C., for example). Carbon molecules having curved surfaces, such as carbon molecules having fullerene bonds, are preferably used in the laser irradiation target. As the carbon molecule having the fullerene bonds, a carbon molecule having a spherical surface, such as the C60molecule, is preferably used. By use of such a laser irradiation target in a laser ablation process, single-wall carbon nanotubes can be formed efficiently in a low temperature process (at 400° C., for example). Catalysts such as Ni and Co (Ni+Co: 5 at %, for example) are preferably used for the efficient formation of the single-wall carbon nanotubes. The manufacturing method can be conducted by use of simple production equipment such as a short pulse-width laser ablation apparatus, therefore, the production of the single-wall carbon nanotubes can be conducted efficiently with a low cost.

REFERENCES:
patent: 5470680 (1995-11-01), Loutfy et al.
patent: 5997832 (1999-12-01), Lieber et al.
patent: 6228498 (2001-05-01), Yokogawa et al.
patent: 10-273308 (1998-10-01), None
patent: 11-116218 (1999-04-01), None
patent: 11-180707 (1999-07-01), None
Pradeep, T. et al. ‘A Novel FeC60Adduct in the Solid State’ in JACS vol. 114 pp. 2272-2273 (1992), no month 1992.*
Thess et al., ‘Crystalline Ropes of Metallic Carbon Nanotubes’ inSciencevol. 273 pp. 483-487 Jul. 26, 1996.*
Roberts & Caseria,Basic Principle of Organic Chemistry2nd ed. 1977 p. 1505, 1977 no month.*
Andreas Thess et al., “Crystalline Ropes of Metallic Carbon Nanotubes”, Science, vol. 273, Jul. 26, 1996, pp. 483-487.
Shunji Bandow et al., “Effect of the Growth Temperature on the Diameter Distribution and Chirality of Single-Wall Carbon Nanotubes”, The American Physical Society, vol. 80, No. 17, Apr. 27, 1998, pp. 3779-3782.
Masako Yudasaka et al., “Roles of Laser Light and Heat in Formation of Single-Wall Carbon Nanotubes by Pulsed Laser Ablation of CxNiyCoy Targets at High Temperature”, The American Physical Society, J. Phys. Chem. B 1998, 102, 10201-10207.
W.K. Maser et al., “Production of High-Density Single-Walled Nanotube Material by a Simple Laser-Ablation Method”, Chemical Physics Letters 292 (1998), pp. 587-593.
F. Kokai et al., “Growth Dynamics of Single-Wall Carbon Nanotubes Synthesized by CO2 Laser Vaporization”, The American Physical Society, J. Phys. Chem. B 1999, 103, pp. 4346-4351.
L.P. Biro, et al., “Growth of Carbon Nanotubes by Fullerene decomposition in the Presence of Transition Metals”, Chemical Physics Letters 306 (1999), pp. 155-162.
A.M. Rao et al., “Diameter-Selective Raman Scattering from Vibrational Modes in Carbon Nanotubes”, Science, vol. 275, Jan. 10, 1997, pp. 187-191.

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Manufacturing method of carbon nanotubes and laser... does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Manufacturing method of carbon nanotubes and laser..., we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Manufacturing method of carbon nanotubes and laser... will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-3451556

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.