Process for the preparation of a poly(paraphenylene terephthalam

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From carboxylic acid or derivative thereof

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1621573, 264232, 524104, 524606, 524718, 528348, C08G 6928

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049594532

ABSTRACT:
A process for producing a fibrous gel composition of poly(paraphenylene terephthalamide) comprising the steps of placing terephthaloyl chloride in reactive contact with paraphenylene diamine in a solution of at least one amide-type polar solvent (e.g. N-methylpyrrolidone), an alkaline earth metal salt and the aliphatic tertiary amine, N-methylpyrrolidine or its hydrochloride. Poly(paraphenylene terephthalamide) papers are prepared by diluting the composition in an amide diluent, blending in a slurry of poly(paraphenylene terephthalamide) fibers in a precipitating mediu, filtering, washing, pressing and drying the mixture.

REFERENCES:
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patent: 3869429 (1975-03-01), Blades
patent: 4011203 (1977-03-01), Konomi et al.
patent: 4072664 (1978-02-01), Konomi et al.
patent: 4511623 (1985-04-01), Yoon et al.
patent: 4579895 (1986-04-01), Cuidard et al.
U.S. Ser. No. 7,213,741, filed June 30, 1988.
Japanese Patent Application No. 52-124099, published Oct. 18, 1977.

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