Multisample dynamic headspace sampler

Measuring and testing – Sampler – sample handling – etc. – Plural parallel systems

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137883, F16K 1122

Patent

active

057082197

ABSTRACT:
Method and apparatus for collecting a large number of outgas samples at the same time. Specimens to be tested for outgassing are placed in throw-away widemouth bottles, and the bottles are placed in cups provide in a heating block. A custom made cap is fastened to each bottle using an O-ring. Each cap is provided with an outgassing sample collecting tube. A source of pure gas such as nitrogen or helium is connected by way of a pressure regulator and a hydrocarbon filter to a manifold. Each of the caps on each bottle is coupled to the manifold by way of a metering valve. An adsorbent is placed in each collecting tube. The gas pressure is set to between 10 and 15 psi. The flow through each collecting tube is set to a predetermined level by adjusting its metering valve and measuring the flow at the exit of the collecting tube using a flowmeter. The healing block is heated by means of a thermal tape used in conjunction with a power supply and a thermocouple inserted into a hole in the heating block. The samples are heated and held at an elevated temperature for a predetermined length of time. After the outgassing test is completed, the collecting tubes are desorbed and analyzed with the appropriate instrumentation.

REFERENCES:
patent: 3018788 (1962-01-01), Perlis
patent: 3092141 (1963-06-01), Stark
patent: 3369405 (1968-02-01), Galegar
patent: 3928711 (1975-12-01), Jakobsen
patent: 5469751 (1995-11-01), Weiss et al.
patent: 5598869 (1997-02-01), Nelson

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