Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing
Patent
1997-07-08
1999-02-23
Shippen, Michael L.
Organic compounds -- part of the class 532-570 series
Organic compounds
Oxygen containing
568841, C07C 2900
Patent
active
058746501
ABSTRACT:
A process for the preparation of 4,4,4-trichlorobutan-1-ol which comprises reacting allyl alcohol with chloroform in the presence of a radical initiator. Preferably the allyl alcohol is added incrementally to the chloroform over the period of the reaction.
REFERENCES:
Ameduri and Boutevin, "Synthesis of Chlorinated Telechelic Oligomers"--Macromolecules, vol. 24:9, 1991, pp. 2475-2484.
Chen et al., "Rearrangements and Conformations of Chloroalkyl Radicals by Electron Spin Resonance"--J. American Chem. Soc., vol. 96:7, 1974, pp. 2201-2208.
Imai et al., "Ring Opening Alkylation of Cyclic Ethers with .alpha.-Halogenoalkyllithiums in the Presence of Boron Trifluoride--Dithyl Ether", J. Chem. Soc., Chem Commun., 1994, pp. 2353-2354.
Burkhard Dianne
Shippen Michael L.
Zeneca Limited
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