Radiant energy – Ionic separation or analysis
Patent
1989-10-17
1990-10-02
Berman, Jack I.
Radiant energy
Ionic separation or analysis
250282, 250288, 250289, H01J 4910
Patent
active
049609912
ABSTRACT:
A multimode ionization source includes a resistive filament aligned with an exit cone orifice. The filament generates electrons that bombard molecules near the orifice. In electron impact mode, a pressure regulator selects a low pressure within an ionization chamber and gaseous analyte is injected through a gas inlet and ionized by electron bombardment. In chemical ionization mode, an intermediate pressure of reagent gas established; electrons ionize the reagent gas. Gaseous analyte is introduced is ionized by the reagent gas through chemical interaction. In thermospray mode, a high pressure is established and heated liquid analyte is introduced into the chamber as a spray which is ionized by ion evaporation; in a thermospray/chemical ionization submode, filament activation supplements ion evaporation. Ions produced in all modes can be directed to a mass analyzer for analysis.
REFERENCES:
patent: 4647772 (1987-03-01), Lewis et al.
patent: 4814612 (1989-03-01), Vestal et al.
patent: 4851700 (1989-07-01), Goodley
Goodley Paul C.
Hansen Stuart C.
Berman Jack I.
Hewlett--Packard Company
Nguyen Kiet T.
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