Chemistry of inorganic compounds – Silicon or compound thereof – Oxygen containing
Patent
1989-12-22
1991-02-26
Straub, Gary P.
Chemistry of inorganic compounds
Silicon or compound thereof
Oxygen containing
423118, 502 85, 502 86, C01B 3328
Patent
active
049960342
ABSTRACT:
In the process for inserting extraneous silicon atoms into lattice sites of zeolite crystals from which aluminum atoms have been extracted, it has been found that the use of more concentrated fluorosilicate salt solutions and shorter contact times between the zeolite crystals and the salt solution than heretofore proposed, enables the production of more highly siliceous products with less defect structure. Advantageously the zeolite crystals are contacted with the concentrated fluorosilicate salt solution in a stepwise manner with the crystals being washed to remove fluoride ions between each contact with the salt solution.
REFERENCES:
patent: 4503023 (1985-03-01), Breck et al.
patent: 4597956 (1986-07-01), Hinchey et al.
patent: 4610856 (1986-09-01), Skeels et al.
patent: 4753910 (1988-06-01), Han et al.
patent: 4840779 (1989-06-01), Cannan
Breneman R. Bruce
McBride Thomas K.
Miller Richard G.
Straub Gary P.
UOP
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