Methods for metal assays using optical techniques

Chemistry: analytical and immunological testing – Metal or metal containing – Li – na – k – rb – cs – fr – be – mg – ca – sr – ba – ra

Reexamination Certificate

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C436S073000, C436S083000, C436S084000

Reexamination Certificate

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08003394

ABSTRACT:
An improved optical method for determining metal or a metal compound thereof in a sample with organic impurities. The optical method comprises of solvating the metal in a liquid medium and then mixing this liquid medium with an optical indicator and then measuring the presence of the metal. The improvement lies in removing any organic impurities by the addition of an additive, where the said additive is removed before the optical indicator is added.

REFERENCES:
patent: 7129093 (2006-10-01), McCleskey et al.
patent: 2005/0280816 (2005-12-01), Agrawal et al.
patent: WO2008130737 (2008-10-01), None
Determination of a Trace Amount of Beryllium in Water Samples by Graphite Furnace Atomic Absorption Spectrometry after Preconcentration and Separation as a Beryllium-Acetylacetonate Comples on Activated Carbon Tadao Okutani, Yasuhiro Tsurunta, Akio Sakuragawa Analytical Chemistry (1993) 65: 1273-1276.
U.S. Appl. No. 12/338,724, filed Dec. 18, 2008.
NIOSH 7704, Manual of Analytical Methods (NMAM), 5th Edition.
NIOSH 9110, Manual of Analytical Methods (NMAM), 5th Edition.
ASTM D7202, Standard Test Method for Deterimination of Beryllium in the Workplace Using Field-Based Extraction and Fluorescence Detection. Oct. 2006.
ASTM D7458, Standard Test Method for Determination of Beryllium in Soil, Rock, Sediment, and Fly Ash Using Ammonium Bifluoride Extraction and Fluorescence Detection. Oct. 2008.
NIOSH 7703, Manual of Analytical Methods (NMAM), 5th Edition.
EPA SW846-7196. Jul. 1996.
NIOSH 7700, Manual of Analytical Methods (NMAM), 4th Edition, May 15, 1996.
Matsumiya, H., Hoshino, H., Yotsuyanagi, T.,A novel fluorescence reagent, 10-hydroxybenzo[h]quinoline-7-sulfonate, for selective determination of beryllium(II)ion at pg cm−3levels, Analyst, vol. 126, pp. 2082-2086 (2001).
Ashley K.; Agrawal, A.; Cronin, J.; Tonazzi, J.; McCleskey, T. M.; Burrell, A. K.; Ehler, D. S.,Ultra-trace determination of beryllium in occupational hygiene samples by ammonium bifluoride extraction and fluorescence detection using hydroxybenzoquinoline sulfonate, Analytical Chimica Acta, vol. 584, pp. 281-286 (2007).
(Agrawal et al-2) Agrawal, A; Cronin, J.; Agrawal, A; Tonazzi, J.; Ashley, K.; Brisson, M.; Duran, B.; Whitney, G.; Burrell, A.; McCleskey, T.M.; Robbins, J.; White, K.,Extraction and Optical Fluorescence Method for the Measurement of Trace Beryllium in Soils. Environmental Science and Technology, vol. 42, pp. 2066-2071 (2008).
Agrawal, Anoop; Cronin, John; Adams, Lori; Agrawal, Akshay; Tonazzi, Juan Carlos;Fluorescence Analysis of Beryllium in Samples Contaminated by Strongly Fluorescent Impurities, Submitted for publication, Journal of Occupational and Environmental Health (Also presented at Third International Symposium on Beryllium Particulates and Their Detection. Organized by Beryllium Health and Safety Committee (Department of Energy) in Albuquerque, New Mexico, 2008).

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