Method for purifying L-glutamine

Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acids and salts thereof

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C07C22700

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active

049669940

ABSTRACT:
L-glutamine is purified by concentrating a fermentation liquor containing at least 40 g/l or more of L-glutamine, or a solution obtained therefrom by filtering off microbial cells, at pH 5.6.+-.0.5, or by cooling the fermentation liquor or the solution after concentration or without concentration at a temperature in the range of 2.degree. to 30.degree. C., thereby giving a slurry of L-glutamine crystals of 70 g/l or higher concentration; (2) separating the crystals from the mother liquor and then dissolving the separated crystals in a water; and (3) bringing the solution thus obtained into contact with an OH-type anion-exchange resin, thereby removing impurities through adsorption.

REFERENCES:
patent: 3206506 (1965-09-01), Griffith
patent: 3886039 (1975-05-01), Yoshinaga

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