Process for purifying removal of acrylic acid, methacrylic...

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

Reexamination Certificate

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C562S600000

Reexamination Certificate

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07947845

ABSTRACT:
A process for purifying removal of acrylic acid, methacrylic acid, N-vinylpyrrolidone or p-xylene crystals from their suspension in mother liquor by means of a wash column with forced transport, whose shell of the process chamber is a metal wall, the wash column additionally being enveloped by a thermal insulation material having a water vapor barrier and a specific heat flow of >0.1 W/m2and <10 W/m2flowing into the process chamber through the metal wall of the wash column.

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P.J. Jansens, et al., “The Purification Process in Hydraulic Packed-Bed Wash Columns”, Chemical Engineering Science, Elsevier Science Ltd., vol. 50, No. 17, 1995, pp. 2717-2729.
D. Verdoes, et al., “Improved Procedures for Separating Crystals from the Melt”, Applied Thermal Engineering, Verlag Elsevier Science Ltd., vol. 17, No. 8-10, 1997, pp. 879-888.
European Search Report dated Aug. 3, 2010, in the corresponding Belgium Application No. BE200800380 (submitted with with English translation of categories).

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