Preparation of biscarbamates and novel biscarbamates

Details Preparation of biscarbamates and novel biscarbamates Preparation of biscarbamates and novel biscarbamates

1987-02-13

1988-07-26

Niebling, John F.

Chemistry: electrical and wave energy

Processes and products

204 72, 560115, C25B 302

Patent

active

047598328

ABSTRACT:
Biscarbamates, including novel one, of the general formula ##STR1## where R is alkyl of 1 to 8 carbon atoms and X is a hydrocarbon radical of 2 to 60 carbon atoms in which one or more carbon atoms may be replaced by hetero atoms and which may contain halogen atoms or ester, carbonyl or nitrile groups are prepared by electrochemically oxidizing formamides of the general formula ##STR2## in the presence of an alkanol of the formula ROH and of an ionic halide.

REFERENCES:
patent: 3226428 (1965-12-01), Vail et al.
patent: 3341568 (1967-09-01), Ham
patent: 3391181 (1968-07-01), Scheuerl
patent: 3950285 (1976-04-01), Wolgemuth
patent: 4118500 (1978-10-01), Mitzlaff et al.
patent: 4430262 (1984-02-01), Engels et al.
patent: 4661217 (1987-04-01), Degner et al.
Tetrahedron 32 (1976), 2815-2206.
Journal of Organic Chemistry 48 (1983) 3338-3339.

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