Process for separating 3-hydroxy steroids or sterols from mixtur

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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C07J 900

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042798280

ABSTRACT:
A process for separating 3-hydroxy steroids from mixtures of lipids by combining a solution of the sterol-containing mixture in isopropanol or other similar alcoholic solvents with a slurry or solution of calcium dichloride in isopropanol or other similar alcoholic solvents. The complexed sterols are isolated by evaporating the alcoholic solvents, washing the residue with a hydrocarbon solvent and filtration. The sterols can be subsequently liberated from the complex by treatment with an aqueous/alcohol and isolated by filtration.

REFERENCES:
patent: 4057541 (1977-11-01), Weber et al.
patent: 4148810 (1979-04-01), Struve

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