Process of preparation of phosphinamides, applications and new p

Details Process of preparation of phosphinamides, applications and new p Process of preparation of phosphinamides, applications and new p

1990-10-17

1991-11-26

Robinson, Allen J.

Organic compounds -- part of the class 532-570 series

Organic compounds

Amino nitrogen containing

564 13, 558207, C07F 936

Patent

active

050684256

ABSTRACT:
Phosphinamides are prepared by the action of an organic halide on an oxazaphospholidine. Depending upon the configuration desired for the stereoisomer to be obtained, an oxazaphospholidine is utilized which has been derived from a (+) or (-) optically-active amino-alcohol. These phosphinamides are useful for the preparation of phosphinates, in particular optically-active phosphinates of known absolute configuration; for this, the phosphinamide is subjected to alcoholysis.

REFERENCES:
Trippettl & Walker, J. Org. Chem., 1960, 25, 2130-2133.
Fujisawa et al., Bulletin of the Chemical Society of Japan, vol. 40, 147-149 (1967).

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