Silicon nitride sintered body and process for preparation thereo

Compositions: ceramic – Ceramic compositions – Refractory

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501 97, 423344, C04B 3558

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active

050175300

ABSTRACT:
A silicon nitride sintered body comprised of 1.5 to 3.0% by weight of Y.sub.2 O.sub.3, 0.1 to 1.0% by weight of Al.sub.2 O.sub.3 and 96 to 98.4% by weight of Si.sub.3 N.sub.4 wherein the Y.sub.2 O.sub.3 /Al.sub.2 O.sub.3 weight ratio is at least 2.5, and having a density of at least 3.0 g/cm.sup.3, exhibits a high oxidation resistance and a high strength at a high temperature. This silicon nitride sintered body is prepared by sintering a powdery mixture consisting essentially of 1.5 to 3.0% by weight of Y.sub.2 O.sub.3 powder, 0.1 to 1.0% by weight of Al.sub.2 O.sub.3 powder, and 96 to 98.4% by weight of Si.sub.3 N.sub.4 powder, the Y.sub.2 O.sub.3 /Al.sub.2 O.sub.3 weight ratio being at least 2.5, the oxygen content in the Si.sub.3 N.sub.4 powder being less than 2.0% by weight and the total metallic impurity content in the Si.sub.3 N.sub.4 being less than 200 ppm, at a temperature of 1,850.degree. to 2,000.degree. C. in a non-oxidizing atmosphere.

REFERENCES:
patent: 3969125 (1976-07-01), Komeya et al.
patent: 4284432 (1981-08-01), Nishida et al.
patent: 4341874 (1982-07-01), Nishida et al.
patent: 4654315 (1987-03-01), Hsien

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