Process for the preparation of 2,4-dihydroxybenzophenones

Distillation: processes – separatory – Vaporization zone under positive pressure or vacuum

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203 38, 203 58, 203 47, 568315, 568322, 568324, B01D 310

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active

045684294

ABSTRACT:
2,4-Dihydroxybenzophenone is prepared substantially quantitatively and in a highly purified form by reacting resorcinol with a benzotrihalide in the presence of an aqueous solution of N-methylpyrrolidone and subsequently subjecting the crude reaction product mixture to vacuum distillation.

REFERENCES:
patent: 2682559 (1954-06-01), Stanley et al.
patent: 2861104 (1958-11-01), Von Glahn
patent: 3526666 (1970-09-01), Ponder
patent: 3830845 (1974-08-01), Arimoto et al.
patent: 3843729 (1974-10-01), Lachmann et al.
patent: 3850988 (1974-11-01), Ruby
Chemical Abstract, vol. 83, 1975, Hireaki et al., "2-Hydroxy-4-(Alkadienyloxy)benzophenones", Abstract No. 78868x, p. 628.

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