Mixture of 1-(2-propenyl)-3-(4-methyl-3-pentenyl)-.DELTA..sup.3

Details Mixture of 1-(2-propenyl)-3-(4-methyl-3-pentenyl)-.DELTA..sup.3 Mixture of 1-(2-propenyl)-3-(4-methyl-3-pentenyl)-.DELTA..sup.3

1977-08-24

1978-10-24

Helfin, Bernard

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

426534, 424 69, C07C 4738

Patent

active

041221222

ABSTRACT:
Described are the compounds 1-(2-propenyl-3-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehyde and 1-(2-propenyl)-4-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehyde; and a process for preparing same by means of reacting an allylic halide with a mixture of 3 and 4-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehyde using a phase transfer agent in a two phase system according to the reaction: ##STR1## wherein the carboxaldehyde moiety is bonded to the alpha-carbon atom or the beta-carbon atom, X is chloro or bromo and M is alkali metal, processes for adding such 1-(2-propenyl)-(4-methyl-3-pentenyl)-.DELTA..sup.3 -cyclohexene-1-carboxaldehydes to consumable materials whereby:

REFERENCES:
patent: 2933506 (1960-04-01), Ohloff
patent: 3929895 (1975-12-01), Hall
patent: 4081483 (1978-03-01), Hall et al.

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