Reductive destruction of nitrosamines, hydrazines, nitramines, a

Details Reductive destruction of nitrosamines, hydrazines, nitramines, a Reductive destruction of nitrosamines, hydrazines, nitramines, a

1983-07-13

1985-08-13

Sutto, Anton H.

Organic compounds -- part of the class 532-570 series

Organic compounds

Chalcogen in the nitrogen containing substituent

564112, 564113, 564415, 564416, 564417, 564418, 564414, 564422, 564448, 564489, 564494, 544358, 546184, 548400, C07D29500, C07C 8511

Patent

active

045351546

ABSTRACT:
A method for the reduction of nitrogen compounds containing an N--N or N.dbd.N bond, which are soluble in water or lower alcohols, particularly nitrosamines, hydrazines, nitramines, azo- and azoxy-compounds, to the corresponding amines; comprising contacting the nitrogen compounds with a hydroxide solution and a nickel-aluminum alloy in the absence of a hydrogen atmosphere, at room temperature and at atmospheric pressure, for a sufficient time to produce the corresponding amine in a single step.

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patent: 4038321 (1977-07-01), Thatcher et al.
Grillot, G. F., "Journal of American Chemical Society", vol. 66, p. 2124 (1944).
Paal, C. & Yao, W., "Berichte", Jahrg. 63, pp. 57-66, (1930).
Smith, "Open Chain Nitrogen Compounds", pp. 478-479 (1966).
Fieser et al., "Reagents for Organic Synthesis", vol. I, pp. 718-720 (1967).
Sidgewicks, "Organic Chemistry of Nitrogen", 3rd Ed., pp. 593-595 (1966).
Seebach, D. & Wykypiel, W., "Synthesis", pp. 423-424 (1979).

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