Preparation of alcohols by treating esters with alkali metal bor

Details Preparation of alcohols by treating esters with alkali metal bor Preparation of alcohols by treating esters with alkali metal bor

1978-01-05

1979-05-29

Mars, Howard T.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

568864, 568885, C07C 3134

Patent

active

041567919

ABSTRACT:
Esters are treated with alkali metal borohydride to produce alcohols. Substantially constant boiling admixtures of: methanol/methyl heptafluorobutyrate, water/1,1-dihydroheptafluorobutanol, and water/methyl heptafluorobutyrate are described.

REFERENCES:
patent: 2662914 (1953-12-01), Robeson
patent: 2683721 (1954-02-01), Schlesinger
patent: 2824897 (1958-02-01), Wujciak et al.
patent: 2839513 (1958-06-01), Ahlbrecht et al.
patent: 2945886 (1960-07-01), Brown
patent: 3277147 (1966-10-01), Machleidt et al.
patent: 3959389 (1976-05-01), Kurata et al.
Foerst, Newer Methods of Preparative Organic Chemistry, vol. IV, 1968, pp. 167, 204-208, Academic Press, N.Y.
Brown et al., J. Org. Chem., 28, pp. 3261-3263, 1963.

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