Process for the manufacture of potassium stabilized silica sols

Compositions – Preservative agents – Anti-corrosion

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252310, 252306, 252302, C09K 1302

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049158708

ABSTRACT:
A method for producing a silica sols containing less than 150 ppm sodium haivng an average particle size of 2-110 nm, and a particle size distribution with a coefficient dispersion of 0.16-0.4. The silica sols are produced using a KOH heal to which aliquots of modified silicic acid containing acidic anions are added. The aliquots are added to maintain a substantially constant concentration of colloidal silica in the product. Subsequent to production, the sols may be concentrated by ultrafiltration.
Preparation of low sodium silica sols utilizing a constant silica technique by heating the initial heel to a temperature greater than 80.degree. C. and adding additional silica maintaining an approximately constant total silica. The stabilization is effected with a KOH.

REFERENCES:
patent: 2577484 (1951-12-01), Rule
patent: 3239521 (1966-03-01), Weldes
patent: 3326910 (1967-06-01), Weldes
patent: 3582494 (1971-06-01), Vossos et al.
patent: 3597248 (1971-08-01), Yates
patent: 3630954 (1971-12-01), Yates
patent: 4054536 (1977-10-01), Schaefer et al.

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