Manufacture of isomer-free 3-methylbutylamine

Details Manufacture of isomer-free 3-methylbutylamine Manufacture of isomer-free 3-methylbutylamine

1975-11-21

1977-07-19

Wyman, Daniel E.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260690, C07C 8506, C07B 100

Patent

active

040368831

ABSTRACT:
Manufacture of 3-methylbutylamine by reacting 2-methylbuten-1-ol-4 with hydrogen and a molar excess of ammonia simultaneously at about 140.degree. to 240.degree. C. at superatmospheric pressure in the presence of a hydrogenation catalyst metal or metals, i.e., the transition metals of Group VIII or copper.

REFERENCES:
patent: 3022349 (1962-02-01), Lemon et al.
patent: 3278598 (1966-10-01), Markiewitz
patent: 3520933 (1970-07-01), Adam et al.
Groggins, "Unit Processes in Organic Synthesis", Fifth Edition, pp. 574-576 (1958).
Jardine et al., "J. Chem. Soc., Org", vol. 4, pp. 458-462 (1966).

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