Extraction of hydroperoxides

Details Extraction of hydroperoxides Extraction of hydroperoxides

1978-03-13

1979-07-03

Lone, Werren B.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

C07C17902

Patent

active

041600002

ABSTRACT:
A hydroperoxide containing reaction mixture also containing a corresponding unreacted hydrocarbon is treated with an aqueous alcoholic solvent, e.g., aqueous methanolic solvent, to provide in a first step an extract containing a high percentage of hydroperoxide and an appreciable amount of original or unreacted hydrocarbon whereupon the extract is treated with water under recited conditions to obtain two desired phases, one of which is primarily hydrocarbon rejected from the extract by the addition of water and the other an aqueous methanolic solution of the desired hydroperoxide suitable for use in the acid-catalyzed decomposition for the production of carbonyl compounds and hydroxy compounds.

REFERENCES:
patent: 2430864 (1947-11-01), Farkas et al.
patent: 2915558 (1959-12-01), Alder et al.

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