Process for hydride transfer reduction rearrangement of 8-exo-hy

Details Process for hydride transfer reduction rearrangement of 8-exo-hy Process for hydride transfer reduction rearrangement of 8-exo-hy

1976-11-26

1977-11-22

O'Keefe, Veronica

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260666M, 260617R, C07C 1354

Patent

active

040596435

ABSTRACT:
The hydride transfer reduction rearrangement of 8-exo-hydroxymethyl-endo-tricyclo [5.2.1.0.sup.2,6 ] decane in the presence of concentrated sulfuric acid and a hydride source provides 4-homoisotwistane (tricyclo [5.3.1.0.sup.3,8 ] undecane).

REFERENCES:
patent: 3976710 (1976-08-01), Takaishi et al.
Naotake Takaishi et al., J. Org. Chem., vol. 41, No. 5, 771-775, 1976.
Naotake Takaishi et al., J. Org. Chem., vol. 40, No. 3, 276-281, 1975.
Naotake Takaishi et al., J. Org. Chem., vol. 40, No. 10, 1483-1487, 1975.

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