Preparation of 2-(hydroxymethyl)-acrylonitrile and 2-(hydroxymet

Details Preparation of 2-(hydroxymethyl)-acrylonitrile and 2-(hydroxymet Preparation of 2-(hydroxymethyl)-acrylonitrile and 2-(hydroxymet

1985-12-03

1987-03-31

Brust, Joseph Paul

Organic compounds -- part of the class 532-570 series

Organic compounds

Nitriles

558372, 558451, 560181, 558 20, C07C12130, C07C 5703

Patent

active

046544321

ABSTRACT:
2-(hydroxymethyl)-acrylonitrile and 2-(hydroxymethyl)-acrylates of the formula ##STR1## where X is --CN or ##STR2## and R is unsubstituted or substituted alkyl, are prepared by reacting acrylonitrile or an acrylate with hydrated formaldehyde or a hemiacetal of formaldehyde in the presence of a tertiary amine as a catalyst.

REFERENCES:
patent: 3066165 (1962-11-01), Rosenthal et al.
patent: 3499024 (1970-03-01), Morita et al.
patent: 3743669 (1973-07-01), Hillman et al.
Weygand/Hilgetag, Preparative Organic Chemistry, (1972), p. 954; John Wiley & Sons, N.Y.-London.

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