Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acid esters
Patent
1995-03-24
1996-06-25
Dees, Jose G.
Organic compounds -- part of the class 532-570 series
Organic compounds
Carboxylic acid esters
562443, 562445, C07C22934
Patent
active
055301550
ABSTRACT:
Addition of a reaction mixture obtained by the mineral acid hydrolysis of at least one side flow generated from the production of .alpha.-L-aspartyl-L-phenylalanine methyl ester to a crystallization slurry containing L-phenylalanine while maintaining the pH of the slurry at 3-8 by adding aqueous alkali affords crystallized L-phenylalanine having a low water content in a high yield.
REFERENCES:
patent: 4803300 (1989-02-01), Hijiya et al.
patent: 5118840 (1992-06-01), Kano et al.
patent: 5304671 (1994-04-01), Abe et al.
Chemical Abstracts, vol. 109, No. 23, p. 710, Dec. 5, 1988, AN 211485u, JP-A-63 159 355, R. Mita, et al., "Recovery of L-Phenylalanine and L-Aspartic Acid from a Process for Aspartame Manufacture".
Hijiya Toyoto
Mochizuki Chiaki
Nagashima Kazutaka
Takemoto Tadashi
Ajinomoto Co. Inc.
Conrad, III Joseph M.
Dees Jos,e G.
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