Preparation of finely-divided refractory powders of groups III-V

Chemistry of inorganic compounds – Boron or compound thereof – Binary compound

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423250, 423251, 423252, 423254, 423256, 423290, 423291, 423297, 423344, 423345, 423346, 423406, 423409, 423411, 423412, 423439, 423440, 423561, C01B 3504, C01B 2106, C01B 3130, C01B 3306

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039795004

ABSTRACT:
The preparation of metal and metalloid carbides, borides, nitrides silicides and sulfides by reaction in the vapor phase of the corresponding vaporous metal halide, e.g., metal chloride, with a source of carbon, boron, nitrogen, silicon or sulfur respectively in a reactor is described. Reactants can be introduced into the reactor through a reactant inlet nozzle assembly. Inhibition and often substantial elimination of product growth on exposed surfaces of such assembly is accomplished by introducing the corresponding substantially anhydrous hydrogen halide, e.g., hydrogen chloride, into the principal reactant mixing zone.

REFERENCES:
patent: 3218205 (1965-11-01), Ruehriwein
patent: 3253886 (1966-05-01), Lamprey et al.
patent: 3399980 (1968-09-01), Bourdeau
patent: 3485586 (1969-12-01), Swaney
patent: 3755541 (1973-08-01), Strepkoff
patent: 3761576 (1973-09-01), Groening
patent: 3848062 (1974-11-01), Steiger et al.

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