Process for preparing 1-fluorocyclopropyl methyl ketone

Details Process for preparing 1-fluorocyclopropyl methyl ketone Process for preparing 1-fluorocyclopropyl methyl ketone

1993-03-02

1994-08-09

Reamer, James H.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

549322, C07C 4554

Patent

active

053368096

ABSTRACT:
A new process for the preparation of 1-fluorocyclopropyl methyl ketone of the formula ##STR1## which process comprises a) in a first step, reacting 2-acetyl-2-chloro-4-butanolide of the formula ##STR2## with an addition product of triethylamine and hydrogen fluoride of the formula

REFERENCES:
patent: 4913727 (1990-04-01), Stroech et al.
Synthesis, International Journal of Methods in Synthetic Organic Chemistry, No. 3, 1977, pp. 189-191.
Tetrahedron Letters, vol. 31, No. 45, Oct. 1990, pp. 6527-6530.
Saburo Takei, Tetrahedron Letters No. 49, 1975, pp. 4389-4392.
M. B. Giudicelli, Tetrahedron Letters, vol. 31, No. 45, 1990, pp. 6527-6530.
Lutz Fitjer, Synthesis, "1,1-Bifunctional Cyclopropanes; Convenient Synthesis of 1-Bromo-, 1-Chloro-, and 1-Fluorocyclopropyl Methyl Ketone," 1977, pp. 189-191.
Chemistry Letters, 1975, p. 1152.

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