Device for nebuilizing sample liquid for spectroscopical purpose

Optics: measuring and testing – By dispersed light spectroscopy – With sample excitation

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356315, 356316, G01N 2172, G01N 2173, G01N 2174

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active

048863599

ABSTRACT:
For nebulizing sample liquid for spectroscopical purposes a liquid to be nebulized is pressurized to a minimum pressure of 30 bar through a high-pressure pump formed as a separate unit, and is nebulized through a nozzle having a smallest flow aperture of less than 5.multidot.10.sup.-9 m.sup.2. The high-pressure pump and the nozzle are interconnected through conduits. In one embodiment the pump takes in pure solvent. The sample is taken in on the high-pressure side through a loop, which is arranged to be connected between pump and nozzle.

REFERENCES:
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patent: 4361401 (1982-11-01), Smith, Jr. et al.
patent: 4517495 (1985-05-01), Piepmeier
patent: 4575609 (1986-03-01), Fassel et al.
Schrenk, W. G., "Historical Development of Flame Excitation Sources for Analytical Spectroscopy", vol. 40, No. 1, 1986, pp. XIX-XXVIII.
Snyder & Kirkland Introduction to Modern Liquid Chromatography, pp. 90-114, 1979 edition.
Welz, Atomabsorptionsspektrometrie, pp. 38-43, 270-271, 1983 edition.
Doherty & Hieftji, "Jet--Impact Nebulization for Sample Introduction in Inductivity Coupled Plasma Spectrometry", 1369 Applied Spectroscopy 38, pp. 405-412, (May/Jun. 1984).

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