Process for the preparation of lactosylurea, its purification an

Organic compounds -- part of the class 532-570 series – Organic compounds – Carbohydrates or derivatives

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536 18, 536 22, 426568, C07H 500

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active

042673143

ABSTRACT:
A process for the preparation of lactosylurea and the N-methylol derivative thereof which are usable as feed supplements for ruminants.
According to this process, lactose and urea are heated to 70.degree.-110.degree. C. with a minimum of water and, if possible, this water is eliminated during the reaction. The crude reaction product can be purified by grinding with ice-water or ethanol and subsequent draining so as to eliminate by dissolution in such solvants the unreacted urea.
The corresponding N-methylol derivative is obtained by the reaction with formaldehyde.

REFERENCES:
patent: 2612497 (1952-09-01), Meijer
patent: 3654200 (1972-04-01), Hsu
patent: 4066750 (1978-01-01), Smith et al.

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