Poly(arylene sulfide) polymer containing sulfone, ether and biph

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From phenol – phenol ether – or inorganic phenolate

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128126, 128128, 128174, 128388, C08G 7500

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active

052450007

ABSTRACT:
Poly(arylene sulfide) polymers containing sulfone, ether and biphenyl groups are prepared by a two step process. In the first step, a diphenol is reacted with either a dihaloaromatic sulfone monomer or a bis(haloarylsulfonyl) biphenyl monomer, or both, in the presence of an alkali metal base and a polar organic compound. In the second step, the reaction mixture above is reacted with a sulfur source, and any monomer which was not employed in the first step, if any. The polymers prepared according to the invention process exhibit increased glass transition temperatures over those of known poly(arylene sulfide) polymers. The structure of repeating units of the polymer can be controlled by varying the sequence of addition of the monomers.

REFERENCES:
patent: 4016145 (1977-04-01), Campbell
patent: 4108837 (1978-08-01), Johnson et al.
patent: 4783520 (1988-11-01), Kelsey et al.
patent: 4808694 (1989-02-01), Edmonds, Jr. et al.
"Polyelhersulfones", Encyclopedia of Chemical Technology, 3rd Edition, vol. 18, pp. 605-610, & 613-615 (1982).
"Polysulfone Resins", Encyclopedia of Chemical Technology, 3rd Edition, vol. 18, pp. 832-847 (1982).
"Poly(aryl Ethers) by Nucleophilic Chromatic Substitution, I. Synthesis and Properties", Johnson et al., Journal of Polymer Science: Part A-1, vol. 5, pp. 2375-2398 (1967).

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