Process for the manufacture of 1,4-bis[2-(4'-carbomethoxystyreny

Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acid esters

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560 76, 568 9, C07C 6700, C07F 954

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active

045379858

ABSTRACT:
A process for the manufacture of 1,4-bis[2-(4'-carbomethoxystyrenyl)] benzene is disclosed. This process comprises reacting, at a temperature of about 0.degree. C. to about 100.degree. C., in a highly polar anhydrous organic solvent or solvent mixture, or in liquid ammonia, a p-xylylene-bis-(trialkylphosphonium halide) or p-xylylene-bis-(triarylphosphonium halide) with 4-carbomethoxybenzaldehyde, initiated by the slow introduction of an organometallic compound or an inorganic base. Polyesters, such as polyethylene terephthalate, are copolymerized with about 5 to about 20 parts per million of 1,4-bis[2-(4'-carbomethoxystyrenyl)] benzene. 1,4-bis[2-(4'-carbomethoxystyrenyl)] benzene is useful to provide permanent whiteness to polyesters and polyamides and other synthetic or natural polymers. Polyesters are useful for the manufacture of fibers, films, and related industrial products.

REFERENCES:
patent: 2612516 (1952-09-01), Heimsch et al.
patent: 3076020 (1963-01-01), Stilz et al.
patent: 3177208 (1965-04-01), Stilz et al.
patent: 4179578 (1979-12-01), Fleck et al.

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