Dicyanotricyclodecane

Details Dicyanotricyclodecane Dicyanotricyclodecane

1977-12-12

1979-04-24

Brust, Joseph Paul

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260453AP, 2604653, 260563P, 528 74, 528272, 528310, 528344, 568817, C07C12002, C07C12146

Patent

active

041511948

ABSTRACT:
A mixture of 3,8- and 4,8-dicyanotricyclo[5.2.1.0]decane is prepared by the hydrocyanation of 8-cyanotricyclo[5.2.1.0]dec-3-ene in the presence of a catalyst system comprising a zero valent nickel complex, free of carbon monoxide, a promoting amount of a metal compound such as zinc chloride and a hydroxy-containing aryl compound such as p-cresol as a solvent.

REFERENCES:
patent: 3778462 (1973-12-01), Taylor et al.
patent: 3925445 (1975-12-01), King et al.
patent: 3928414 (1975-12-01), Shimizu et al.
patent: 3960920 (1976-06-01), Ohotsubo
patent: 3992433 (1976-11-01), Ariyoshi et al.
patent: 4076748 (1978-02-01), Hoffmann et al.
Brown, et al., Preprint, A.C.S. Meeting, Minneapolis, Minn., Apr.-1969, pp. B29-B34.

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