Process for the preparation of chloromethyl methyl ether

Details Process for the preparation of chloromethyl methyl ether Process for the preparation of chloromethyl methyl ether

1975-07-15

1976-08-03

Mars, Howard T.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260476R, 260488R, C07C 4100

Patent

active

039729478

ABSTRACT:
Single vessel, closed system, anhydrous, process for preparing high purity chloromethyl methyl ether comprising reacting methylal with hydrogen chloride; wherein said hydrogen chloride is generated, in situ, by contacting methanol, a reaction intermediate, with an acid chloride.

REFERENCES:
patent: 3086060 (1963-04-01), Greer
Kirk Othmer, Encyclopedia of Chemical Technology, John Wiley, New York, 2nd Ed. 1966, p. 96.
Baeyer, Ber 6, (1873), p. 221.
Buehler et al., Survey of Organic Synthesis, John Wiley, New York, 1970, pp. 310-311.

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