Method of and apparatus for outgassing raw material used to grow

Chemistry: physical processes – Physical processes

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Details

23295R, 23305A, 422290, 423600, 423625, C22B 905, C30B 2920

Patent

active

043057250

ABSTRACT:
A method and apparatus for outgassing raw materials includes the steps of and means for heating the material to a temperature of about 800.degree. C. and maintaining that temperature for a first bake out period during which the material is maintained at a pressure of about 200 millitorr and for a second bake out period during which the material is maintained at a pressure of about 5 millitorr or less. During the first bake out period, an inert gas is backstreamed through the raw material.

REFERENCES:
patent: 3011870 (1961-12-01), Webb et al.
patent: 3608050 (1971-09-01), Carman et al.
patent: 3922872 (1975-12-01), Reilly et al.
patent: 3960503 (1976-06-01), Rice
patent: 3998686 (1976-12-01), Meiling et al.

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