Process for preparing 10,11-dihydro-11-exo-hydroxy-5-methyldiben

Details Process for preparing 10,11-dihydro-11-exo-hydroxy-5-methyldiben Process for preparing 10,11-dihydro-11-exo-hydroxy-5-methyldiben

1988-06-24

1989-09-26

Niebling, John F.

Chemistry: electrical and wave energy

Processes and products

204 73R, 204 78, 204 59R, C25B 300

Patent

active

048697915

ABSTRACT:
10,11 Dihydro-11-exo-hydroxy-5-methyldibenzo[a,d]cyclohepten-5,10-imine is prepared in a four step synthesis which uses an electrochemical cyclization to form the 5,10-imine bridge in about a 50% yield.

REFERENCES:
patent: 4399141 (1983-08-01), Anderson et al.
Baizer et al., "Organic Electrochemistry", 2nd ed., Marcel Dekker Inc., New York, pp. 534-541, (1983).

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