Preparation of water-soluble organic silicon compounds

Details Preparation of water-soluble organic silicon compounds Preparation of water-soluble organic silicon compounds

1996-09-06

2000-06-20

Shaver, Paul F.

Organic compounds -- part of the class 532-570 series

Organic compounds

Silicon containing

556413, 427387, 4273936, 427397, C07F 710

Patent

active

060779667

ABSTRACT:
Water-soluble organic silicon compounds are prepared by effecting co-hydrolysis of (A) 1-30 parts of an alkyltrialkoxysilane of R.sup.1 Si(OR.sup.2).sub.3 or a partial hydrolyzate thereof, (B) 70-90 parts of an alkoxy-containing siloxane of R.sup.3.sub.a (OR.sup.2).sub.b SiO.sub.(4-a-b)/2, and (C) 1-20 parts of an amino-containing alkoxysilane of R.sup.4 R.sup.5 NR.sup.6 --SiR.sup.7.sub.n (OR.sup.2).sub.3-n or a partial hydrolyzate thereof in the presence of an organic or inorganic acid. R.sup.1 is a C.sub.7 -C.sub.18 alkyl group, R.sup.2 is a C.sub.1 -C.sub.4 alkyl group, R.sup.3 is a C.sub.1 -C.sub.6 alkyl group, R.sup.4 and R.sup.5 are a hydrogen atom, C.sub.1 -C.sub.15 alkyl or aminoalkyl group, R.sup.6 is a divalent C.sub.1 -C.sub.18 hydrocarbon group, and R.sup.7 is a C.sub.1 -C.sub.4 alkyl group. Letters a and b are 0.75.ltoreq.a.ltoreq.1.5, 0.2.ltoreq.b.ltoreq.2, and 0.95<a+b<3.4. These water-soluble organic silicon compounds are fully water soluble and shelf stable and can be used as an agent for preventing porous materials from water absorption simply after dilution with water. Porous materials are coated or impregnated with the compounds so that they are given excellent water repellency and water absorption-preventing effect.

REFERENCES:
patent: 5077421 (1991-12-01), Selvig
patent: 5087715 (1992-02-01), Snow
patent: 5276123 (1994-01-01), King et al.
patent: 5567752 (1996-10-01), Stein et al.

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