Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From ketone or ketene reactant
Patent
1990-05-22
1992-02-18
Anderson, Harold D.
Synthetic resins or natural rubbers -- part of the class 520 ser
Synthetic resins
From ketone or ketene reactant
528223, 528224, 528226, 528388, 528494, 528495, 528496, 528497, 528498, 528499, C08G 218, C08G 7516
Patent
active
050895966
ABSTRACT:
Aromatic sulfide/ketone polymer is prepared from dihaloaromatic ketone, alkali metal sulfide, water and a polar organic compound. The polymerization reaction mixture comprising the aromatic sulfide/ketone polymer is subjected to a heat soak at elevated temperature then a separation agent (non-solvent) is added under controlled conditions and subsequently cooled to provide a mixture comprising particulate aromatic sulfide/ketone polymer.
Biaxially-oriented film is made from recovered particles of aromatic sulfide/ketone polymer prepared as described by (1) washing the polymer particles with an aqueous calcium salt, (2) heating said washed particles to remove water, wherein the resulting heated particles are at least partially crystalline, (3) molding said heating particles to form a sheet of polymer, (4) biaxially stretching said sheet above the glass transition temperature of the polymer to form a film, and (5) heat-setting said biazially-oriented film under stretching tension for a time and at a temperature to increase strength properties and density.
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Bobsein Rex L.
Cliffton Michael D.
Geibel Jon F.
Reed Jerry O.
Anderson Harold D.
Dollar Beverly M.
Phillips Petroleum Company
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