Process for the preparation of n-methylmorpholine oxide

Details Process for the preparation of n-methylmorpholine oxide Process for the preparation of n-methylmorpholine oxide

1992-01-27

1993-06-01

Ramsuer, Robert W.

Organic compounds -- part of the class 532-570 series

Organic compounds

Four or more ring nitrogens in the bicyclo ring system

C07D29524

Patent

active

052161544

ABSTRACT:
N-methylmorpholine oxide which is essentially free from nitrosamine contaminants is prepared by oxidizing a feedstock consisting essentially of N-methylmorpholine with an oxidant consisting essentially of aqueous hydrogen peroxide in an atmosphere consisting essentially of carbon dioxide to thereby form a nitrosamine-free reaction product from which N-methylmorpholine oxide essentially free from nitrosamine can be recovered.

REFERENCES:
EPA 0 307 184 (Bauer et al.) (Mar. 1989) Chem. Abts. 111:114,735.

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