Preparation of 4-homoisotwistane, (tricyclo[5.3.1.0.sup.3,8 ]und

Details Preparation of 4-homoisotwistane, (tricyclo[5.3.1.0.sup.3,8 ]und Preparation of 4-homoisotwistane, (tricyclo[5.3.1.0.sup.3,8 ]und

1978-01-23

1979-01-09

O'Keefe, Veronica

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260666M, C07C 1328

Patent

active

041338405

ABSTRACT:
A process for the hydride transfer reduction rearrangement of tricyclo[6.2.1.0.sup.2,6 ]undeca-2(6)-ene having the formula (I): ##STR1## by subjecting tricyclo[6.2.1.0.sup.2,6 ]undeca-2(6)-ene having the formula (I) to rearrangement with concentrated sulfuric acid in the presence of a hydride source to convert it to 4-homoisotwistane (tricyclo[5.3.1.0.sup.3,8 ]undecane) having the formula (II): ##STR2##

REFERENCES:
naotaki Takaishi et al., J. Org. Chem. 40, 276, 1483, 2929, 1975.
Naotaki Takaishi et al., J. Org. Chem. 41, 771, 1976.

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