Continuous process for the production of powdered polyisocyanate

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – At least one aryl ring which is part of a fused or bridged...

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528 44, 528 45, 528 59, 528 85, 528902, C08G 1880

Type

Patent

Status

active

Patent number

049407503

Description

ABSTRACT:
The present invention is directed to a continuous process for the production of powdered polyisocyanate addition products in finely divided form which by simultaneously (a) mixing a polyisocyanate component, an isocyanate-reactive component and an inert organic medium containing a surfactant, wherein at least one of the components is insoluble in the inert organic medium, in a low shear stator-rotor dynamic mixer operating at speeds of about 300 to 8000 rpm, utilizing a mixing wattage of about 0.05 to 10.0 watts per cubic centimeter and having a mixing volume of at least about 0.1 liters and (b) reacting the polyisocyanate component with the isocyanate reactive-reactive component in the inert organic medium to form solid polyisocyanate addition products which can be separated from the inert organic medium to form a powder, the average residence time of the components and the inert organic medium in the dynamic mixer being about 3 to 300 seconds and the overall flow rate through the dynamic mixer being at least about 20 kg/h.
The present invention is also directed to the powdered polyisocyanate addition products produced by this process.

REFERENCES:
patent: 3787525 (1974-01-01), McGarr
patent: 3817886 (1974-01-01), McGarr
patent: 3917741 (1975-11-01), McGarr
patent: 3933759 (1976-01-01), Hoeschele
patent: 3963710 (1976-06-01), Aufdermarsh, Jr.
patent: 4680367 (1987-07-01), Kopp et al.

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