Process for the purification of epoxy compounds

Details Process for the purification of epoxy compounds Process for the purification of epoxy compounds

1977-02-04

1980-11-11

Milestone, Norma S.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07D30132

Patent

active

042332028

ABSTRACT:
The low molecular water-soluble onium-catalyst dissolved in the liquid mixture of epoxy resin and excess epihalohydrin obtained by the reaction in the presence of base of a compound having --OH, --SH, --COOH or .dbd.NH groups with excess 1-halo-2,3-epoxyalkane, is separated therefrom by contacting the liquid mixture, either prior to or after separation therefrom of the precipitated salt produced by the reaction, with at least about 5 parts by weight based on the weight of the catalyst present in the liquid mixture, of an adsorbent containing or capable of absorbing at least 1% by weight of water so strongly that it cannot be removed either by drying over concentrated sulfuric acid or by drying at 110.degree. C. and can only be partially removed by drying at 200.degree. C. under vacuum (about 1 millibar), and then separating the adsorbent with catalyst adsorbed thereon from the liquid mixture.

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