Process for the manufacture of 1,1,1,2-tetrafluorochloroethane a

Organic compounds -- part of the class 532-570 series – Organic compounds – Halogen containing

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570134, 570137, 570165, C07C 1708

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053549287

ABSTRACT:
The invention relates to a process for the manufacture of 1,1,1,2-tetrafluorochloroethane and of pentafluoroethane.
The process which consists of gas phase catalytic fluorination of at least one pentahaloethane of formula C.sub.2 HX.sub.2-n F.sub.3+n in which X denotes a chlorine or bromine atom and n the number 0 or 1, by hydrofluoric acid, is characterized in that a catalyst is employed consisting of a catalytic quantity of chromium in an oxidation state equal to or greater than 3 and of an activated charcoal as support.
The selectivity for 1,1,1,2-tetrafluorochloroethane and pentafluoroethane reaches approximately 95% and even more.

REFERENCES:
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patent: 4129603 (1978-12-01), Bell
patent: 4766260 (1988-08-01), Manzer et al.
patent: 4843181 (1989-06-01), Gumprecht et al.
Patent Abstracts of Japan, vol. 9, No. 91 (C-277) (1814) Apr. 19, 1985 59-225131(A).
Patent Abstracts of Japan, vol. 5, No. 75 (C-55) (747) May 19, 1981 56-24050(A).
European Search Report dated Jan. 30, 1991.

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