Process for the preparation of 1-nitroalkene

Details Process for the preparation of 1-nitroalkene Process for the preparation of 1-nitroalkene

1981-07-06

1983-05-17

Shaver, Paul F.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

C07B 1100

Patent

active

043841490

ABSTRACT:
A process for the preparation of 1-nitroalkene which comprises the reaction of a 1-alkene with dinitrogen tetroxide in the presence of oxygen and an ether solvent to form an alkene-dinitrogen tetroxide adduct and subsequent reaction of the resulting adduct with sodium fluoride in the presence of an inert gas.

REFERENCES:
patent: 1872700 (1932-08-01), Dreyfus
patent: 2384048 (1945-09-01), Smith et al.
patent: 2478243 (1949-08-01), Coe et al.
patent: 3510531 (1970-05-01), Larkin et al.

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