Process for the preparation of o-carboethoxybenzenesulfonamide

Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acid esters

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C07C14367

Patent

active

045714290

ABSTRACT:
Saccharin is reacted with ethanol and concentrated sulfuric acid. Sodium acetate is used to remove saccharin from the crude material so that highly pure o-carboethoxybenzene sulfonamide is recovered.

REFERENCES:
patent: 2946815 (1960-07-01), Hamor
patent: 3008928 (1961-11-01), Rueggeberg
patent: 3399123 (1968-08-01), Passal
Loev, J. Org. Chem., 27, pp. 1703-1709 (1962).

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