Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acid esters
Patent
1985-05-03
1986-02-18
Shippen, Michael L.
Organic compounds -- part of the class 532-570 series
Organic compounds
Carboxylic acid esters
C07C14367
Patent
active
045714290
ABSTRACT:
Saccharin is reacted with ethanol and concentrated sulfuric acid. Sodium acetate is used to remove saccharin from the crude material so that highly pure o-carboethoxybenzene sulfonamide is recovered.
REFERENCES:
patent: 2946815 (1960-07-01), Hamor
patent: 3008928 (1961-11-01), Rueggeberg
patent: 3399123 (1968-08-01), Passal
Loev, J. Org. Chem., 27, pp. 1703-1709 (1962).
E. I. Du Pont de Nemours and Company
Shippen Michael L.
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